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Protic solutions were 80% ethanol-water by weight. , and acetic acid from Mallinckrodt Chemical Co. (Paris, Kentucky) as specified in the text. Adjustment of pH was made with potassium hydroxide or hydro chloric acid. Electrolysis experiments and cyclic voltammetry were performed with an ςς adder" type operational amplifier potentiostat (28) constructed at the electronics facility of the Chemistry Department, Northwestern Univer sity. The potentiostat was used together with a voltage generator which provided a reference voltage of either a constant voltage or a triangular wave form with 1 mV incremental steps.